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81.
The adsorption and thermal analysis of 1-propanamine has been compared over MFI zeolites which contain H, Ga, and In cations. In the case of H+-containing materials, NH3 and propene are simultaneously desorbed above 600 K. This behavior, is well known and characteristic of the Hofmann elimination reaction. However, a distinctly different mode of reaction is observed in the case of Ga and In containing materials. NH3 is released below 600 K, propene and other products are released above 600 K, and a stable residue remains above 800 K. It is suggested that such behavior results from Lewis acid interactions of Ga or In cations with propanamine.On leave from the Bulgarian Academy of Sciences, Institute of Organic Chemistry. 相似文献
82.
Montmorillinite clays, modified with either Zn(II) or Fe(III) chlorides have been used to catalyze the Friedel-Crafts alkylation of thiophene. High yields (ca. 80%) of 2- and 3-benzylthiophene mixtures were obtained using either catalyst in chlorobenzene or nitrobenzene solvent at 80°C. The ratio of 2–3-products was found to be controlled by their relative stability. Reactions were most rapid in nitrobenzene solution (<5 min) and resulted in formation of the 2-isomer as the only mono-substituted product. This is believed to be the first example in which an alkylation of thiophene has been limited to one regio-isomer. 相似文献
83.
对连续流动法测定硫化物进行初步探讨和研究。同时与其他几种测定硫化物的方法进行了比较。实验结果表明,连续流动法对硫化物分析在线性、稳定性、最低检测限、准确性和精密度等方面均优于其他方法。 相似文献
84.
对宁夏炼油厂一台200m3低合金钢球罐H2S应力腐蚀裂纹采用气刨打磨后补焊的返修方法表明,碳弧气刨时的骤热不会使裂纹向纵深扩展,只是必须在补焊前将返修部位焊缝两侧各100mm范围内打磨至完全露出金属光泽,以便彻底消除裂纹源,避免补焊时再产生新的微小裂纹。若返修深度不大于罐壁厚度的二分之一,则不必进行射线探伤检查,只须进行100%的超声波检查,在水压试验前后对返修部位进行100%磁粉探伤则是非常必要的。 相似文献
85.
86.
R Venkataraghavan K M Satyalakshmi K S R K Rao A K Sreedhar M S Hegde H L Bhat 《Bulletin of Materials Science》1996,19(1):123-129
Single crystalline oriented films of indium antimonide have been grown on cadmium telluride substrates by the pulsed laser
deposition technique. The films were (111) oriented which is the substrate orientation. The composition of the grown films
were found to deviate from that of the target owing to loss of antimony during evaporation. This deviation from stoichiometry
led to film-substrate reaction, resulting in mixed interface. The antimony deficiency in the films were controlled by correcting
the stoichiometry, which led to avoiding mixed interfaces. The stoichiometric films showed good surface morphology and well
defined sharp interfaces. The IR transmission spectrum showed sharp band to band absorption and effective detection in the
MWIR.
Paper presented at the poster session of MRSI AGM VI, Kharagpur, 1995 相似文献
87.
We have made a study of the chemical composition, the electrical, the optical and the structural properties of polycrystalline CuInS2 thin films prepared by spray pyrolysis to be used for thin film solar cells. These films were deposited starting from aqueous solutions with different chemical compositions ([Cu]/[In] and [S]/[Cu] ratios) and at different substrate temperatures. In all cases, the material is p-type with grains preferentially oriented in the (112) direction of the sphalerite structure. The electro-optical properties show a very strong dependence on the [Cu]/[In] ratio in the solution. Films with copper excess have smaller resistivity and better crystallinity than those which are stoichiometric or have indium excess. The results obtained in this work show the possibility of having CuInS2 thin films with a wide range of resistivity, a fact that could be important for making solar cells based on this material. 相似文献
88.
添加尖晶石对氧化锌压敏电阻性能的影响 总被引:1,自引:0,他引:1
通过添加尖晶石(Zn7Sb2O(12))改性研制出电位梯度为100V/mm左右,压敏电压在82~150V,通流容量可达1600A/cm2,漏电流<2μA系列压敏电阻器,从而满足了国内电话交换机行业对82V、100V、120V、150V压敏电阻器的电性能要求。从工艺的角度解释了尖晶石对氧化锌瓷晶粒的作用原理,并分析了尖晶石的微观结构及粒度对瓷片电性能的影响。 相似文献
89.
90.
从废旧锌锰电池中回收锌和锰的工艺研究 总被引:1,自引:0,他引:1
高玉华 《有色金属再生与利用》2006,(7):19-20
废旧锌锰干电池经过剖开、焙烧处理,去除汞和碳粉,再用硫酸浸取,滤液采用沉淀法分离锌和锰。锌和锰的回收率分别为94.5%和93.6%。 相似文献